HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-Methyl-N(4-t-Butylphenylthiosulfenyl) Carbamoyl Fluoride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Tert-Butylbenzenethiol | HCID 75454 | — |
| Reactant | N-methyl-N-chlorothiocarbamoyl fluoride | HCID 20327306 | — |
| Reactant | N-methyl-N-(4-chlorophenylthiosulfenyl)carbamoyl fluoride | HCID 23333002 | — |
| Solvent | Pentane | HCID 8003 | — |
| Product | N-Methyl-N(4-t-Butylphenylthiosulfenyl) Carbamoyl Fluoride | HCID 23333006 | — |
Reaction Steps
Prepared by reacting 0.5 g of 4-t-butylthiophenol in pentane with 0.44 g of N-methyl-N-chlorothiocarbamoyl fluoride. The reaction proceded with a vigorous exotherm and evolution of hydrochloric acid gas. The infrared and n.m.r. spectra of the product was identical to the material prepared by Method I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04091016 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-fa71a60d6f244171a56e63b8bc36ee36 |
| Source note | uspto-grants-1978_05 |