HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenol → HCID 22767921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenol | HCID 9732 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Chloro-5-nitrobenzaldehyde | HCID 72933 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22767921 | HCID 22767921 | — |
Reaction Steps
448 G. of 4-fluoro-phenol and 742 g. of 2-chloro-5-nitro-benzaldehyde are added to a solution of 184 g. of sodium hydroxide in 7.4 liters of water. The mixture is then left to cool to room temperature. The precipitate is removed by filtration, washed carefully with water, and there is obtained 2-(4-fluoro-phenoxy)-5-nitro-benzaldehyde, having a melting point of 125°-126° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04091023 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-950b743091094f8cbc654ca4e6dc3df2 |
| Source note | uspto-grants-1978_05 |