HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 53963722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 9989489 | HCID 9989489 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53963722 | HCID 53963722 | 99.3% |
Reaction Steps
A solution of 22.7 g of monomethylamine in 160 ml of benzene was added to a solution of 40 g of 5-oxo-8,9-dihydro [5H] benzocycloheptene in 400 ml of ethanol and the mixture was stirred for 2 1/2 hours and was evaporated to dryness to obtain 47.5 g of 7-methylamino-5-oxo-6,7,8,9-tetrahydro [5H] benzocycloheptene which was used as is for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04091115 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-8f1b9237e1e2402aab465292866b6386 |
| Source note | uspto-grants-1978_05 |