HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 3-(4-Chlorophenyl)-6-hydrazinylpyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 3-Chloro-6-(4-chlorophenyl)pyridazine | HCID 12257502 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | 3-(4-Chlorophenyl)-6-hydrazinylpyridazine | HCID 12726863 | — |
Reaction Steps
A mixture of 10.0 g. of 6-(p-chlorophenyl)-3-chloropyridazine, 6.6 g. of hydrazine hydrate and 150 ml. of butanol is heated at reflux overnight. The reaction mixture is cooled and the precipitate is collected by filtration, washed with butanol and water and then dried yielding 6-(p-chlorophenyl)-3-hydrazinopyridazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04092311 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-b0b02fcee0a44c98a5d896154f42a7c5 |
| Source note | uspto-grants-1978_05 |