HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 14273121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | 3-Chloro-6-phenylpyridazine | HCID 88515 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 14273121 | HCID 14273121 | — |
Reaction Steps
A mixture of 10.0 g. of 6-phenyl-3-chloropyridazine 7.8 g. of methylhydrazine and 75 ml. of n-butanol is refluxed 6 hours. The mixture is cooled and filtered to give product and the filtrate is concentrated and filtered to give additional product. The two crops of product are recrystallized from ethanol to give crystals, m.p. 145°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04092311 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-69ff6bf7740a4699944668cce1b36406 |
| Source note | uspto-grants-1978_05 |