HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 20326505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Reactant | 3-Chloro-6-(4-cyanophenyl)pyridazine | HCID 6405256 | — |
| Product | HCID 20326505 | HCID 20326505 | — |
Reaction Steps
A mixture of 5.0 g. of 6-(p-cyanophenyl)-3-chloropyridazine, 8.71 g. of t-butylcarbazate and 100 ml. of butanol are heated at reflux for 3 hours. The solvent is removed on a rotating evaporator. Water is added, the resulting product is recovered by filtration, washed with water, recrystallized from methanol and dried yielding a product having a m.p. 169°-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04092311 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-c516913a396b493e8b42d2093d3671e1 |
| Source note | uspto-grants-1978_05 |