HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 20326515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | 3-Chloro-6-(4-chlorophenyl)pyridazine | HCID 12257502 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 20326515 | HCID 20326515 | — |
Reaction Steps
A 10.0 g. portion of 6-(p-chlorophenyl)-3-chloropyridazine and 6.1 g. of methyl hydrazine in 125 ml. of butanol is mixed and heated at reflux overnight. The reaction mixture is cooled, filtered, the precipitate is washed with butanol and water and dried. Recrystallization from ethanol gives 6-(p-chlorophenyl)-3-(1-methylhydrazino)pyridazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04092311 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-e6eeeb061844403eb548b7221439e666 |
| Source note | uspto-grants-1978_05 |