1-Butanol → HCID 20326523, compound

Participants

Reaction Steps

To an 8.0 g. portion of 5-methyl-6-(m-nitrophenyl)-3-chloropyridazine in 100 ml. of butanol is added 4.4 g. of methyl hydrazine. This reaction mixture is heated at reflux overnight and then cooled in an ice bath. The product which forms as a precipitate is collected by filtration, washed with butanol, water, dried and recrystallized from ethanol, m.p. 173°-174° C.

Provenance & Evidence