HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazinoethanol → HCID 20326524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazinoethanol | HCID 8017 | — |
| Reactant | 3-Chloro-6-(4-chlorophenyl)pyridazine | HCID 12257502 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 20326524 | HCID 20326524 | — |
Reaction Steps
A mixture of 5.0 g. of 6-(p-chlorophenyl)-3-chloropyridazine and 5.02 g. of 2-hydroxyethylhydrazine in 75 ml. of butanol is heated at reflux overnight and then cooled in an ice bath. The precipitate is collected by filtration, washed with butanol, water and then dried. Recrystallization from ethanol gives crystals, m.p. 172°-174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04092311 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-6e692fb99758431eaf2478f41e5a82b0 |
| Source note | uspto-grants-1978_05 |