HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 20326522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | 3-Chloro-6-(4-cyanophenyl)pyridazine | HCID 6405256 | — |
| Product | HCID 20326522 | HCID 20326522 | — |
Reaction Steps
A mixture of 7.5 g. of 6-(p-cyanophenyl)-3-chloropyridazine, 3.5 g. of methylhydrazine and 75 ml. of n-butanol is refluxed for 3 hours. The mixture is cooled and filtered to give the product. Recrystallization from dioxane gives 6-(p-cyanophenyl)-5-methyl-3-(1-methylhydrazino)pyridazine as tan crystals, m.p. 149°-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04092311 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-f5a3b4e5cee24c29b352fc488ea0515f |
| Source note | uspto-grants-1978_05 |