HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 53899950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 20327149 | HCID 20327149 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53899950 | HCID 53899950 | — |
Reaction Steps
In the manner of Example II, 22.1 g of 3-phenoxybenzyl 4-bromo-6,6,6-trichlorohexanoate was treated with 7.4 g of piperidine. Chromatography of the crude reaction product on a charcoal column using benzene as the eluent gave 13.5 g of 3-phenoxybenzyl 3,3-dimethyl-6,6,6-trichloro-4-hexenoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04092482 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-81b9c944d55345e6998fbc7e629942ca |
| Source note | uspto-grants-1978_05 |