反应详情

A solution of 19.23 grams (0.10 mol) of the N-(2-dimethylaminoethyl)benzamide, prepared as described in Example 1, 12.66 grams (0.10 mol) of α-chlorotoluene and 64 milliters of acetonitrile was heated at reflux for 19.75 hours. Solid crystallized on cooling which was collected, washed with acetonitrile and dried. The yield of product was 24.0 grams (75.27% of theory); mp=175°-176° C.

1. temperaturewas heated
2. temperatureat reflux for 19.75 hours
3. customSolid crystallized
4. temperatureon cooling which
5. customwas collected
6. washwashed with acetonitrile
7. customdried