HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → N,N-Dimethyl-N-(2-benzoylaminoethyl)benzylammonium Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | N-(2-(Dimethylamino)ethyl)benzamide | HCID 113158 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N,N-Dimethyl-N-(2-benzoylaminoethyl)benzylammonium Chloride | HCID 19811098 | — |
Reaction Steps
A solution of 19.23 grams (0.10 mol) of the N-(2-dimethylaminoethyl)benzamide, prepared as described in Example 1, 12.66 grams (0.10 mol) of α-chlorotoluene and 64 milliters of acetonitrile was heated at reflux for 19.75 hours. Solid crystallized on cooling which was collected, washed with acetonitrile and dried. The yield of product was 24.0 grams (75.27% of theory); mp=175°-176° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05162188 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-80630acfb6e64d19be126317e4c1d130 |
| Source note | uspto-grants-1992_11 |