Ethyl Acrylate → HCID 19811166, compound

HRID 372947Notes

Reaction equation

HRID 372947 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][NH:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:19]([O:23][CH2:24][CH3:25])(=[O:22])[CH:20]=[CH2:21]>>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][N:11]([CH2:21][CH2:20][C:19]([O:23][CH2:24][CH3:25])=[O:22])[CH2:12][C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 8821Ethyl AcrylateHCID 22024852HCID 22024852, compound

Product 1

HCID 19811166HCID 19811166, compound

Procedure

Starting from N-(4-phenylbutyl)-N-benzylamine and ethyl acrylate, ethyl 3-[N-(4-phenylbutyl)-N-benzylamino]-propionate is obtained analogously to Example 1 and is hydrolyzed with hydrochloric acid to give 3-[N-(4-phenylbutyl)-N-benzylamino]-propionic acid hydrochloride, melting point 145°-147°.

Sources & evidence

ORD record
ord-aca8ac43f37f4342851827db2112a84e
Source dataset
uspto-grants-1992_11
Patent number
US05162310

Reaction notes

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