HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67841292, compound → HCID 21614768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67841292 | HCID 67841292 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21614768 | HCID 21614768 | — |
Reaction Steps
27.13 g (0.085 mol) of this hydrochloride are hydrogenated in 300 ml of ethanol over 3 g of 5% palladium-on-charcoal catalyst at 20°-25° under normal pressure until the uptake of hydrogen has ended. The catalyst is filtered off with suction, the filtrate is evaporated and the residue is crystallized from acetone. 3-[N-(4-Phenylbutyl)-amino]-propionic acid hydrochloride is obtained, melting point 135°-137°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05162310 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-c627d1651f6b43628d76fc6da56f658c |
| Source note | uspto-grants-1992_11 |