反应详情

This compound was prepared according to the general method of Example 90 using 2,2'-dithiobisbenzoyl chloride (3.00 g, 8.74 mmol) in 75 mL of dichloromethane and 4-aminopyrimidine (1.66 g, 17.5 mmol) in 14 mL of pyridine. The crude product was triturated with a hot mixture of acetonitrile and DMF, filtered, and recrystallized from water-DMF to yield 0.08 g of the title compound, mp 234°-235° C.

1. customThis compound was prepared
2. customThe crude product was triturated with a hot mixture of acetonitrile and DMF
3. filtrationfiltered
4. customrecrystallized from water-DMF