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HRID373069

反应详情

EQUATION

反应方程式

HRID 373069 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CN(C)CCn1c(=O)[nH]c2ccccc21
HCID14894678

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCn1c(=O)[nH]c2ccccc21.Cl
HCID19811396

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

To a solution of 1,3-dihydro-1-(2-dimethylaminoethyl)-2H-benzimidazol-2-one (1.32 g) in ether (40 ml) was added 4N hydrogen chloride in dioxane dropwise with stirring. The separated crystals were collected by suction and dried to give 930 mg of 1,3-dihydro-1-(2-dimethylaminoethyl)-2H-benzimidazol-2-one hydrochloride.

WORKUP

后处理

  1. customThe separated crystals were collected by suction
  2. customdried