HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dimethyl-5-ethoxycarbonylbarbituric acid → HCID 19811558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dimethyl-5-ethoxycarbonylbarbituric acid | HCID 593714 | — |
| Reactant | HCID 14819451 | HCID 14819451 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19811558 | HCID 19811558 | — |
Reaction Steps
14.50 g (40.6 mmol) of 4-(2-(1,1,2,2,3,3-hexafluoropropoxy)-1,1,2-trifluoroethoxy)-aniline were added to 9.26 g (40.6 mmol) of 1,3-dimethyl-5-ethoxycarbonylbarbituric acid in 100 ml of toluene, the mixture was stired under reflux for 2.5 hours and concentrated and the residue was recrystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05162327 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-df7e9aa50fd54996b8f60d7cfc04b264 |
| Source note | uspto-grants-1992_11 |