Triethylamine → HCID 131717619, compound

Participants

Reaction Steps

2.25 g (3.34 mmol) of 1,3-dimethyl-5-(3,5-dichloro-(4-(2-(1,1,2,2,3,3,3-heptafluoropropoxy)-1,1,2-trifluoroethoxy))-phenylcarbamoyl)-barbituric acid in 30 ml of acetonitrile were stirred with 0.38 g (3.7 mmol) of triethylamine at room temperature for 2 hours. The solution was concentrated and the residue was dried at 50° C. under an oil pump vacuum.

Provenance & Evidence