HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azido(trimethyl)stannane → HCID 178441453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azido(trimethyl)stannane | HCID 5104973 | — |
| Reactant | 2-Butyl-6-methyl-3-[[4-(2-cyanopyridin-3-yl)phenyl]methyl]quinazolin-4(3H)-one | HCID 19811513 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178441453 | HCID 178441453 | — |
Reaction Steps
A solution of the product of step C (1.0 eq.) is added trimethylstannylazide (3 eq.) in toluene (3 mL) and heated to reflux for 36 h. The mixture is cooled to rt, concentrated and then can be purified by flash chromatography on SiO2 to give the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05162325 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-880b91e67ef84260867a78725a778a89 |
| Source note | uspto-grants-1992_11 |