Trichloroisocyanuric Acid → HCID 19811969, compound

HRID 373158Notes

Reaction equation

HRID 373158 reaction equation
ClN1[C:7](=[O:8])[N:6]([Cl:9])[C:5](=O)N(Cl)C1=O.[Cl:13][CH2:14][CH:15]1[O:19]C(=O)NC1>C(Cl)Cl>[Cl:9][N:6]1[CH2:5][CH:15]([CH2:14][Cl:13])[O:19][C:7]1=[O:8]

Participants

4

Reactant 2

HCID 6909Trichloroisocyanuric AcidHCID 908155-Chloromethyloxazolidin-2-one

Product 1

HCID 19811969HCID 19811969, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

8.4 grams (0.036 moles) trichloroisocyanuric acid were dissolved in dried methylene chloride. To this suspension were added 5 grams (0.036 moles) 5-Chloromethyl-2-oxazolidinone. The mixture was stirred for several hours before filtering to remove solids. The methylene chloride layer was rotovaped to recover the product, a yellow liquid Proton NMR Data: δ3.7 (m, 4 protons), 4.8(m, 1 proton). Elemental analysis Chlorine found 39.66 (theory 41.7).

Workup

  1. filtrationbefore filtering
  2. customto remove solids
  3. customto recover the product

Sources & evidence

ORD record
ord-ac6fc95849e748eaaf895239ecb392c2
Source dataset
uspto-grants-1992_11
Patent number
US05162354

Reaction notes

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