HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroisocyanuric Acid → HCID 19811969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroisocyanuric Acid | HCID 6909 | — |
| Reactant | 5-Chloromethyloxazolidin-2-one | HCID 90815 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19811969 | HCID 19811969 | — |
Reaction Steps
8.4 grams (0.036 moles) trichloroisocyanuric acid were dissolved in dried methylene chloride. To this suspension were added 5 grams (0.036 moles) 5-Chloromethyl-2-oxazolidinone. The mixture was stirred for several hours before filtering to remove solids. The methylene chloride layer was rotovaped to recover the product, a yellow liquid Proton NMR Data: δ3.7 (m, 4 protons), 4.8(m, 1 proton). Elemental analysis Chlorine found 39.66 (theory 41.7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05162354 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-ac6fc95849e748eaaf895239ecb392c2 |
| Source note | uspto-grants-1992_11 |