HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 5-[(4-Methoxyphenyl)-methyl]-2,3-dihydro-1H-benzimidazole-2-thione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | HCID 19812006 | HCID 19812006 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 5-[(4-Methoxyphenyl)-methyl]-2,3-dihydro-1H-benzimidazole-2-thione | HCID 19811998 | — |
Reaction Steps
To a solution of 0.51 g (5.0 mmoles) of triethyl amine, 1.14 g (5.0 mmoles) of 4-[(4-methoxyphenyl)-methyl]-o-phenylene-diamine and 35 ml of chloroform a solution of 0.58 g (5.0 mmoles) of thiophosgene and 10 ml of chloroform are added dropwise.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05162359 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-8fd4664bd01349fba7bd46dbc45f237f |
| Source note | uspto-grants-1992_11 |