Triethylamine → HCID 19811998, compound

HRID 373164Notes

Reaction equation

HRID 373164 reaction equation
C(N(CC)CC)C.[CH3:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([CH2:16][C:17]2[CH:22]=[CH:21][C:20]([NH2:23])=[C:19]([NH2:24])[CH:18]=2)=[CH:12][CH:11]=1.[C:25](Cl)(Cl)=[S:26]>C(Cl)(Cl)Cl>[CH3:8][O:9][C:10]1[CH:11]=[CH:12][C:13]([CH2:16][C:17]2[CH:22]=[CH:21][C:20]3[NH:23][C:25](=[S:26])[NH:24][C:19]=3[CH:18]=2)=[CH:14][CH:15]=1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 10040ThiophosgeneHCID 19812006HCID 19812006, compound

Product 1

HCID 19811998HCID 19811998, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent2×

Procedure

To a solution of 0.51 g (5.0 mmoles) of triethyl amine, 1.14 g (5.0 mmoles) of 4-[(4-methoxyphenyl)-methyl]-o-phenylene-diamine and 35 ml of chloroform a solution of 0.58 g (5.0 mmoles) of thiophosgene and 10 ml of chloroform are added dropwise.

Sources & evidence

ORD record
ord-8fd4664bd01349fba7bd46dbc45f237f
Source dataset
uspto-grants-1992_11
Patent number
US05162359

Reaction notes

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