HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19812359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 10401503 | HCID 10401503 | — |
| Product | HCID 19812359 | HCID 19812359 | — |
Reaction Steps
1 g 3-Cyano-2-morpholino-5,4'-bipyridine-1'-oxide is dissolved in 5 ml 2N HCl and mixed under cooling with isopropanol and ether, filtered off with suction and dried at 100° C. Yield: 0.9 g (79.8% of the theoretical yield), with a melting point of 222° C.-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05162533 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-cf9c751a9c25442c8f844523fd4d709b |
| Source note | uspto-grants-1992_11 |