Hydrochloric Acid → HCID 19812359, compound

HRID 373309Notes

Reaction equation

HRID 373309 reaction equation
[C:1]([C:3]1[C:4]([N:16]2[CH2:21][CH2:20][O:19][CH2:18][CH2:17]2)=[N:5][CH:6]=[C:7]([C:9]2[CH:14]=[CH:13][N+:12]([O-:15])=[CH:11][CH:10]=2)[CH:8]=1)#[N:2].C(O)(C)C.CCOCC.[ClH:31]>>[ClH:31].[C:1]([C:3]1[C:4]([N:16]2[CH2:21][CH2:20][O:19][CH2:18][CH2:17]2)=[N:5][CH:6]=[C:7]([C:9]2[CH:10]=[CH:11][N+:12]([O-:15])=[CH:13][CH:14]=2)[CH:8]=1)#[N:2]

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 3776IsopropanolHCID 10401503HCID 10401503, compound

Product 1

HCID 19812359HCID 19812359, compound

Procedure

1 g 3-Cyano-2-morpholino-5,4'-bipyridine-1'-oxide is dissolved in 5 ml 2N HCl and mixed under cooling with isopropanol and ether, filtered off with suction and dried at 100° C. Yield: 0.9 g (79.8% of the theoretical yield), with a melting point of 222° C.-223° C.

Workup

  1. additionmixed
  2. filtrationfiltered off with suction
  3. customdried at 100° C
  4. customYield: 0.9 g (79.8% of the theoretical yield), with a melting point of 222° C.-223° C.

Sources & evidence

ORD record
ord-cf9c751a9c25442c8f844523fd4d709b
Source dataset
uspto-grants-1992_11
Patent number
US05162533

Reaction notes

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