Glycerol → HCID 19812355, compound

Participants

Reaction Steps

300 mg Potassium hydroxide is dissolved in 15 ml glycerin with heating and 1 g 2-chloro-3-cyano-5,4'-bipyridine-1'-oxide is subsequently added. The reaction mixture is heated for 3 hours at 80° C.-90° C. with stirring, allowed to cool and treated with water. The precipitate obtained is filtered off with suction. Yield: 2 g (89.5% of the theoretical yield), having a melting point of 194° C.-196° C.

Provenance & Evidence