HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 1-(4-Methoxyethoxymethoxyphenyl)-2-hydroxy-1-propanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
| Reactant | 1-Methyl-2-(4'-allyloxy-phenyl)-2-keto-ethyl 4'-heptylbiphenyl-4-ylcarboxylate | HCID 19810057 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-(4-Methoxyethoxymethoxyphenyl)-2-hydroxy-1-propanone | HCID 57263560 | — |
Reaction Steps
To this compound, 0.5 g of PPTS and 100 ml of ethanol were added, and the resulting mixture was stirred at room temperature. After addition of water, the mixture was extracted with toluene. The organic layer thus obtained was neutralized, washed with water, dried, and then concentrated to obtain the desired (S) 1-(4-methoxyethoxymethoxyphenyl)-2-hydroxy-1-propane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05164112 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-1573c6f6679b442a8460970fa997c9e7 |
| Source note | uspto-grants-1992_11 |