HRID373462
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To this compound, 0.5 g of PPTS and 100 ml of ethanol were added, and the resulting mixture was stirred at room temperature. After addition of water, the mixture was extracted with toluene. The organic layer thus obtained was neutralized, washed with water, dried, and then concentrated to obtain the desired (S) 1-(4-methoxyethoxymethoxyphenyl)-2-hydroxy-1-propane.
WORKUP
后处理
- extractionthe mixture was extracted with toluene
- customThe organic layer thus obtained
- washwashed with water
- customdried
- concentrationconcentrated
- customto obtain the