HRID373462

反应详情

EQUATION

反应方程式

HRID 373462 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To this compound, 0.5 g of PPTS and 100 ml of ethanol were added, and the resulting mixture was stirred at room temperature. After addition of water, the mixture was extracted with toluene. The organic layer thus obtained was neutralized, washed with water, dried, and then concentrated to obtain the desired (S) 1-(4-methoxyethoxymethoxyphenyl)-2-hydroxy-1-propane.

WORKUP

后处理

  1. extractionthe mixture was extracted with toluene
  2. customThe organic layer thus obtained
  3. washwashed with water
  4. customdried
  5. concentrationconcentrated
  6. customto obtain the