HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 178471888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | Ethylorthoformate | HCID 53630039 | — |
| Reactant | HCID 53702410 | HCID 53702410 | — |
| Product | HCID 178471888 | HCID 178471888 | — |
Reaction Steps
The resulting compound (28.4 g) was treated with ethyl orthoformate and acetic anhydride to convert it into ethyl 3-ethoxy-2-(2',3',4',6'-tetrafluorobenzoyl)acrylate and this compound was then treated with cyclopropylamine to give 32.8 g of ethyl 3 -cyclopropylamino-2-(2',3',4',6'-tetrafluorobenzoyl)acrylate. m.p. 107°-108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05164392 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-a5652745488b4d5ca44d3117a14c458c |
| Source note | uspto-grants-1992_11 |