HRID373601

反应详情

EQUATION

反应方程式

HRID 373601 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of benzyl 6-benzoyloxy-hexanoate (c) (38.09 g) in ethyl acetate was added 5% Pd/C (3 g) and the resultant mixture was stirred under a hydrogen atmosphere for 24 hours. The crude product obtained by treating in the conventional manner was distilled under reduced pressure (1 mmHg, 182°-192° C.) to give the title compound (d).

WORKUP

后处理

  1. customThe crude product obtained
  2. additionby treating in the conventional manner
  3. distillationwas distilled under reduced pressure (1 mmHg, 182°-192° C.)