HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 373644Generated: October 31, 2026
HCID 13131507, compound → HCID 928691, compound
https://huagongshe.com/reaction/373644
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 13131507 | HCID 13131507 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 928691 | HCID 928691 | — |
Reaction Steps
The crude product D-Phe-Gly-OMe (6 g, 25 mmol) was powdered and then dispersed in 100 ml toluene and heated at reflux overnight. The reaction flask was cooled to 0° C. and the solid product (3.50 9, 69%) was collected by filtration: m.p. 256°-257° C.; DCI-NH3 -MS, m/z (relative intensity), 222 (MNH4+, 100%), 205 (MH+, 31%);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05164388 |
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| Source dataset | uspto-grants-1992_11 |
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| ORD ID | ord-11281c44a8cc4b8c9efeba6f5d979863 |
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| Source note | uspto-grants-1992_11 |
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