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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 373999Erstellt: 26. Oktober 2026

N-Phenylmaleimide → HCID 19808687, Verbindung

https://huagongshe.com/reaction/373999

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN-PhenylmaleimideHCID 13662—
Edukt2-[1-(2,4-Dichlorophenyl)vinyl]indoleHCID 19808719—
LösungsmittelO-XyleneHCID 7237—
ProduktHCID 19808687HCID 1980868750%

Reaktionsschritte

7 ml of xylene was added to a mixture of 1.5 g of 2-[1-(2,4-dichlorophenyl)vinyl]indole and 1.0 g of N-phenylmaleimide. The resulting mixture was refluxed for 1 hour. The solvent was removed by distillation under reduced pressure. The residue was recrystallized from isopropyl alcohol to obtain 1.2 g (yield: 50%) of N-phenyl-1-(2,4-dichlorophenyl)-1,2,3,4-tetrahydro-carbazole-3,4-dicarboximide as colorless crystal.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05166204
Quelldatensatzuspto-grants-1992_11
ORD IDord-0fd4b345d32a4e4f90cdd944df9f8b30
Quellennotizuspto-grants-1992_11