HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Phenylmaleimide → HCID 19808687, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Phenylmaleimide | HCID 13662 | — |
| Edukt | 2-[1-(2,4-Dichlorophenyl)vinyl]indole | HCID 19808719 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | HCID 19808687 | HCID 19808687 | 50% |
Reaktionsschritte
7 ml of xylene was added to a mixture of 1.5 g of 2-[1-(2,4-dichlorophenyl)vinyl]indole and 1.0 g of N-phenylmaleimide. The resulting mixture was refluxed for 1 hour. The solvent was removed by distillation under reduced pressure. The residue was recrystallized from isopropyl alcohol to obtain 1.2 g (yield: 50%) of N-phenyl-1-(2,4-dichlorophenyl)-1,2,3,4-tetrahydro-carbazole-3,4-dicarboximide as colorless crystal.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05166204 |
| Quelldatensatz | uspto-grants-1992_11 |
| ORD ID | ord-0fd4b345d32a4e4f90cdd944df9f8b30 |
| Quellennotiz | uspto-grants-1992_11 |