HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 19808761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 6481892 | HCID 6481892 | — |
| Product | HCID 19808761 | HCID 19808761 | 60% |
Reaction Steps
400 mg of N-(2-dimethylaminoethyl)-6-chlorocarbazole-3,4-dicarboximide, 50 mg of 60% sodium hydride and 150 mg of dimethyl sulfate were subjected to the same reaction as in Example 3 (1) to obtain 250 mg (yield: 60%) of N-(2-dimethylaminoethyl)-6-chloro-9-methylcarbazole-3,4-dicarboximide as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05166204 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-3e607f9a37ad491dbe9772722901f384 |
| Source note | uspto-grants-1992_11 |