HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 19808715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 6481892 | HCID 6481892 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19808715 | HCID 19808715 | 78% |
Reaction Steps
In 10 ml of N,N-dimethylformamide was dissolved 200 mg of N-(2-dimethylaminoethyl)-6-chlorocarbazole-3,4-dicarboximide. Thereto was added 830 mg of methyl iodide. The mixture was stirred at room temperature for 2 hours. The resulting crystals were collected by filtration, washed with ethyl acetate, and dried to obtain 220 mg (yield: 78%) of N-(2-tri methylammonioethyl)-6-chlorocarbazole-3,4-dicarboximide iodide as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05166204 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-7ecaf629985e4c709078a408f5ffc501 |
| Source note | uspto-grants-1992_11 |