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HRID374097

反应详情

EQUATION

反应方程式

HRID 374097 的结构方程式

REACTANTS

反应物

4
结构：O=C(n1ccnc1)n1ccnc1
HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

结构：O=[N+]([O-])c1cnc(Cl)cc1Cl
HCID12275765

2,4-dichloro-5-nitropyridine

C5H2Cl2N2O2

结构：OCCCCNc1ccccc1
HCID13755485

未命名化合物

结构：c1cn(Cc2ncc[nH]2)cn1
HCID19358846

2-(1H-Imidazol-1-ylmethyl)-1H-imidazole

C7H8N4

PRODUCTS

生成物

1
结构：O=c1[nH]c2cnc(N(CCCCO)c3ccccc3)cc2n2c(Cn3ccnc3)ncc12
HCID19809415

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

Treat 2,4-dichloro-5-nitropyridine with 2-((imidazol-1-yl)methyl)imidazole followed by reaction with N-phenyl-4-hydroxybutylamine, hydrogenation with palladium on carbon and cyclization with carbonyldiimidazole to provide the title compound.