HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 6-Acetylbenzothiazolinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | Benzothiazolinone | HCID 53400715 | — |
| Product | 6-Acetylbenzothiazolinone | HCID 131717621 | — |
Reaction Steps
To a solution containing 0.5 mol of anhydrous aluminium chloride in 0.20 mol of dimethylformamide is added 0.05 mol of benzothiazolinone, then, slowly and with agitation, 0.06 mol of acetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05166353 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-1a451a7f8dbb4a2ba62b603aac1c8702 |
| Source note | uspto-grants-1992_11 |