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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 374300Generated: October 31, 2026

HCID 19809645, compound → HCID 19809647, compound

https://huagongshe.com/reaction/374300

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19809645HCID 19809645—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 19809647HCID 19809647—

Reaction Steps

A solution of 11.2 g (39.5 mmol) of 1 butoxy-2,5-dimethyl-4-(phenylmethoxy)benzene (Example L) in 100 mL of methanol containing 1 g of 20% palladium on carbon is shaken under three atmospheres of hydrogen for 1 hour. The catalyst is removed and the solvent evaporated in vacuo to afford 7.6 g of the title compound; mp 43°-45° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05166398
Source datasetuspto-grants-1992_11
ORD IDord-bfb306d4100147fabc2339e8015e88f7
Source noteuspto-grants-1992_11