HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19809645, compound → HCID 19809647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19809645 | HCID 19809645 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19809647 | HCID 19809647 | — |
Reaction Steps
A solution of 11.2 g (39.5 mmol) of 1 butoxy-2,5-dimethyl-4-(phenylmethoxy)benzene (Example L) in 100 mL of methanol containing 1 g of 20% palladium on carbon is shaken under three atmospheres of hydrogen for 1 hour. The catalyst is removed and the solvent evaporated in vacuo to afford 7.6 g of the title compound; mp 43°-45° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05166398 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-bfb306d4100147fabc2339e8015e88f7 |
| Source note | uspto-grants-1992_11 |