HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 53733250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | HCID 18996929 | HCID 18996929 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 53733250 | HCID 53733250 | — |
Reaction Steps
A mixture of 3-cyclopropyl-1-(3,5-dichloropyridin-2-yl)propan-1,3-dione (1.3 g) and N,N-dimethylformamide dimethyl acetal (1.1 ml) in 1,4-dioxane was stirred at room temperature for 4 days and the solvent was evaporated to yield 3-cyclopropyl-1-(3,5-dichloropyridin-2-yl)-2-dimethylaminomethylenepropan-1,3-dione (1.73 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05480857 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-5c40c8bec8a94fbd9840686df03987dd |
| Source note | uspto-grants-1996_01 |