HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131719234, compound → HCID 131719235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131719234 | HCID 131719234 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131719235 | HCID 131719235 | 22% |
Reaction Steps
A solution of 2 g of the crude compound of Example 18 (8.23 mmol), solubilized in 80 ml of anhydrous ethanol, is refluxed for one hour. After evaporation and purification on silica gel (eluent: 35% MeOH/5% H2O/CH2Cl2 then 40% MeOH/5% H2O/CH2Cl2) 400 mg are obtained with a yield of 22%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05480884 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-ce11621bc76449b489bd76617c543be8 |
| Source note | uspto-grants-1996_01 |