HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11405654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 15281822 | HCID 15281822 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 11405654 | HCID 11405654 | 85.2% |
Reaction Steps
A solution of 2.0 g of methyl 4-[3-(4-nitrophenyl)-2-oxooxazolidin-5-yl]methoxybenzoate (compound 50) obtained in Example 3 in 18 ml of acetic acid and 6 ml of concentrated hydrochloric acid was refluxed with heating for 12 hours. After ice-cooling the reaction solution, ether was added thereto and the crystals formed were collected by filtration. Thus, 1.64 g of the title compound (compound 81) was obtained (yield 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05480899 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-f2df8096df16417891bb31bbdc40acbe |
| Source note | uspto-grants-1996_01 |