HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 15281826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 15281825 | HCID 15281825 | — |
| Product | HCID 15281826 | HCID 15281826 | 99% |
Reaction Steps
A 1.2 ml quantity of anhydrous acetic acid was added dropwise to an acetic acid (60 ml) solution of 3.0 g of methyl 4-[3-(4-aminophenyl)-2-oxooxazolidin-5-yl]methoxybenzoate obtained in Example 9 at room temperature, and the mixture was stirred at the same temperature for 1 hour. The crystals were collected by filtration and washed with ethanol to give 3.05 g of the title compound (compound 113) in a yield of 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05480899 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-141cabd3e8464d939d06a2bc9083bd9c |
| Source note | uspto-grants-1996_01 |