HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 15813877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-methylpropyn-2-ylamine | HCID 96160 | — |
| Reactant | Bromopropylphthalimide | HCID 21958088 | — |
| Product | HCID 15813877 | HCID 15813877 | — |
Reaction Steps
A mixture of bromopropylphthalimide (15.51 g, 0.058 mol), N-methyl-N-propargyl amine (5.0 g, 0.()72 mol), potassium carbonate (12.0 g, 0.087 mol), and toluene (40 ml) was refluxed for 4 hours, filtered and the insoluble washed with toluene. After removal of the solvent, the residue was dried in vacuo to provide 14.3 g of title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05480988 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-62facbb4a3504fe28f0cbf79017b884e |
| Source note | uspto-grants-1996_01 |