HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 178442495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Ethyl 3-oxononanoate | HCID 245601 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Product | HCID 178442495 | HCID 178442495 | — |
Reaction Steps
3-n-Hexylisoxazol-5(4H)-one is obtained in 99% yield as a reddish liquid by holding ethyl 3-oxo-pelargonate at reflux temperature for 1 hour with one equivalent of hydroxylamine hydrochloride and one equivalent of pyridine and thereafter working-up in the usual manner.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05481001 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-833c89ff312e4ef4b0916e2c0fd87540 |
| Source note | uspto-grants-1996_01 |