HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → 2,3-Dichloro-4-fluorobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 2,3-Dichloro-4,4'-difluorobenzophenone | HCID 18997584 | — |
| Product | 4-Fluorophenol | HCID 9732 | 60% |
| Product | 2,3-Dichloro-4-fluorobenzoic acid | HCID 10330705 | 78% |
Reaction Steps
If the procedure is as described in Example 13, except that 50.1 g (0.175 mol) of 2,3-dichloro-4,4'-difluorobenzophenone and 10 g of 90 percent hydrogen peroxide, solution are used, 11.8 g (0.105 mol, 60%) of 4-fluorophenol and 28.3 g (0.136 mol, 78%) of 2,3-dichloro-4-fluorobenzoic acid are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05481032 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-96707dabb51a42a0bc4ab36dc61aea06 |
| Source note | uspto-grants-1996_01 |