HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethoxybenzoyl chloride → 2-(2-Ethoxybenzamido)-3-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethoxybenzoyl chloride | HCID 3016397 | — |
| Reactant | 2-Amino-3-methylbenzamide | HCID 14221807 | — |
| Product | 2-(2-Ethoxybenzamido)-3-methylbenzamide | HCID 18536599 | — |
Reaction Steps
The title compound was prepared from 2-amino-3-methylbenzamide (Chem. Pharm. Bull., 1988, 36, 2955) and 2-ethoxybenzoyl chloride following the procedure of Preparation 5 and was obtained as colorless crystals (71%), m.p. 197°-200° C. Found: C,68.80; H,5.99; N,9.36. C17H18N2O3 requires C,68.44; H,6.08; N,9.39%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05482941 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-b2fd3165b0224357bf996d9e9cdaaf9b |
| Source note | uspto-grants-1996_01 |