Bromine → HCID 54395198, compound

Participants

Reaction Conditions

Reaction Steps

24 g of finely powdered 2-nitro-4-trifluoromethylmercapto-aniline were dissolved in 50 ml of trifluoroacetic acid, and 18 g of bromine were metered in at 20° C. The mixture was then subsequently stirred at 20° C. for 3 hours and at 40° C. for a further 30 minutes and poured onto water, and the product was taken up in methylene chloride. After removal of the solvent, 31 g of 6-bromo-2-nitro-4-trifluoromethylmercapto-aniline were obtained.

Provenance & Evidence