HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorine → HCID 53829400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | 2-Nitro-4-(trifluoromethanesulfonyl)aniline | HCID 4529469 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 53829400 | HCID 53829400 | 95.3% |
Reaction Steps
27 g of 2-nitro-4-trifluoromethylsulphonyl-aniline were chlorinated with 10 g of chlorine in 100 ml of acetic acid analogously to Example 14. 29 g of 2-nitro-4-trifluoromethylsulphonyl-6-chloro-aniline were obtained, melting point: 138°-39° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05482956 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-c008ce5723f84c369529c3acd22e8d62 |
| Source note | uspto-grants-1996_01 |