HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18996341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Dibromomalonamide | HCID 175375 | — |
| Reactant | 5-(3-Chlorophenyl)-3-(2-(3,4-dihydroxyphenyl)-1-methylethyl)-2-oxazolidinone | HCID 15669204 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 18996341 | HCID 18996341 | — |
Reaction Steps
One equivalent of 5-(3-chlorophenyl) -3-(2-(3,4-dihydroxyphenyl)-1-methylethyl )-2-oxazolidinone, prepared by the procedure of U.S. Pat. No. 5,061,727; Example 1, one equivalent of dibromomalonamide, acetonitrile, and 4 equivalents of potassium carbonate are stirred at room temperature for 18 hours. The reaction mixture is filtered and evaporated in vacuo to give 5-(2-(5-(3-chlorophenyl)-2-oxo-3-oxazolidinyl)propyl)-1,3 -benzodioxole-2,2-dicarboxamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05482971 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-ec25c2c0d20840a7bbf12546cf75b605 |
| Source note | uspto-grants-1996_01 |