Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2-Bromo-3,4-diethoxycarbonyl-5-nitro-6-phenylpyridine | HCID 19935615 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15289697 | HCID 15289697 | — |
Reaction Steps
In 25 ml of ethanol was dissolved 550 mg of 2-bromo-3,4-diethoxycarbonyl-5-nitro-6-phenylpyridine, whereto 0.36 g (5 eq.) of reduced iron was added, followed by heating to 60° C. After 1.5 ml (16 eq.) of acetic acid was added dropwise, the mixture was refluxed for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05420275 |
|---|
| Source dataset | uspto-grants-1995_05 |
|---|
| ORD ID | ord-98d021ae1c9a43bb964f4d1eb95679d9 |
|---|
| Source note | uspto-grants-1995_05 |
|---|
